Triple channel, fluorine observe and variable temperature spectrometer facilities at different magnetic field strengths have been explored to give as much complementary information as possible. For both chlorinated and fluorinated diazadiphosphetidines, motional properties have been examined and the indirect spin spin and dipolar interactions, together with shielding have been studied. Spectra from the NMR active nuclei in these cyclic dimers have been used to compare effects of differing substituents on NMR properties.
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